GSTDTAP  > 地球科学
DOI10.1126/science.aao0865
Atomic-resolution transmission electron microscopy of electron beam-sensitive crystalline materials
Zhang, Daliang1; Zhu, Yihan2,4; Liu, Lingmei2; Ying, Xiangrong2; Hsiung, Chia-En2; Sougrat, Rachid1; Li, Kun1; Han, Yu2,3
2018-02-09
发表期刊SCIENCE
ISSN0036-8075
EISSN1095-9203
出版年2018
卷号359期号:6376页码:675-+
文章类型Article
语种英语
国家Saudi Arabia; Peoples R China
英文摘要

High-resolution imaging of electron beam-sensitive materials is one of the most difficult applications of transmission electron microscopy (TEM). The challenges are manifold, including the acquisition of images with extremely low beam doses, the time-constrained search for crystal zone axes, the precise image alignment, and the accurate determination of the defocus value. We develop a suite of methods to fulfill these requirements and acquire atomic-resolution TEM images of several metal organic frameworks that are generally recognized as highly sensitive to electron beams. The high image resolution allows us to identify individual metal atomic columns, various types of surface termination, and benzene rings in the organic linkers. We also apply our methods to other electron beam-sensitive materials, including the organic-inorganic hybrid perovskite CH3NH3PbBr3.


领域地球科学 ; 气候变化 ; 资源环境
收录类别SCI-E
WOS记录号WOS:000425117700038
WOS关键词METAL-ORGANIC FRAMEWORK ; CRYO-EM ; DAMAGE ; RECONSTRUCTION ; NANOCRYSTALS ; TEMPERATURE ; GRAPHENE ; SURFACE ; TEM
WOS类目Multidisciplinary Sciences
WOS研究方向Science & Technology - Other Topics
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文献类型期刊论文
条目标识符http://119.78.100.173/C666/handle/2XK7JSWQ/197951
专题地球科学
资源环境科学
气候变化
作者单位1.KAUST, Imaging & Characterizat Core Lab, Thuwal 239556900, Saudi Arabia;
2.KAUST, Adv Membranes & Porous Mat Ctr, Phys Sci & Engn Div, Thuwal 239556900, Saudi Arabia;
3.KAUST, KAUST Catalysis Ctr, Phys Sci & Engn Div, Thuwal 239556900, Saudi Arabia;
4.Zhejiang Univ Technol, Dept Chem Engn, Hangzhou 310014, Zhejiang, Peoples R China
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GB/T 7714
Zhang, Daliang,Zhu, Yihan,Liu, Lingmei,et al. Atomic-resolution transmission electron microscopy of electron beam-sensitive crystalline materials[J]. SCIENCE,2018,359(6376):675-+.
APA Zhang, Daliang.,Zhu, Yihan.,Liu, Lingmei.,Ying, Xiangrong.,Hsiung, Chia-En.,...&Han, Yu.(2018).Atomic-resolution transmission electron microscopy of electron beam-sensitive crystalline materials.SCIENCE,359(6376),675-+.
MLA Zhang, Daliang,et al."Atomic-resolution transmission electron microscopy of electron beam-sensitive crystalline materials".SCIENCE 359.6376(2018):675-+.
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